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BSD-PHM Multi Components HIGH PRESSURE GAS SORPTION ANALYZER

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Key Feature

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Pressure

0-50/69MPa

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Temperature

-196℃ to 1100℃

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Main Function

High pressure Isotherm, PCT, Automatic Cyclic Test

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Optional Function

Kinetics, TPD, TPA,
PCT with larger sample volume (100g level)

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Full Automation

Automatically switches from pre-treatment to testing

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Thermostatic design

The analyzer pipeline temperature is 40.0℃ ±0.1℃.

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Sample cell options

Stainless steel sample cell :2ml/ 5ml/25ml;
Core sample
cell:Φ25.4×50mm/Φ50×110mm/Φ38.1×100mm

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High-pressure design

All stainless steel gas circuit system, the joints are hard-connected with VCR, which improves the stability of the instrument.

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Transducers

High precision with 0.01%FS, long term 0.025%FS;

Specifications

SpecificationsDetails
Main FunctionHigh pressure adsorption and desorption isotherm
High pressure PCT
Automatic Cyclic Test
Optional FunctionIsobaric adsorption/desorption kinetics
Temperature programmed desorption (TPD)
Temperature programmed adsorption (TPA)
Vacuum desorption
PCT test with larger sample volume (100g level)
Analysis station1/2
Degassing station1/2
Pressure0-20MPa
Temperature-196 to 1100℃
Transducer2x pcs 10bar and 200bar with 0.01% full scale
Vacuum10-2 Pa by oil pump
10-8 Pa by molecular pump
Analysis gasH2、CH4、Ar、CO2、N2、Kr、O2、C2H6、C2H4、He etc.
Repeatability±2% by standard sample
Sample cellStainless steel sample cell :2ml/ 5ml/25ml;
Core sample cell:Φ25.4×50mm/Φ50×110mm/Φ38.1×100mm
Self-sealing sample tube
AutomationAutomatically switches from pre-treatment to testing after setup
Instrument thermostatic temperatureThe inside of the instrument is in the same air bath environment, the thermostatic temperature is 40.0℃, and the temperature control accuracy is ±0.1℃.
High-pressure gas pipelineAll stainless steel gas circuit system, the joints are hard-connected with VCR, which improves the stability of the instrument.
Filling rod with filterStandard sample tube filling rod with filtering function can effectively reduce the free space volume of the sample tube and prevent the sample from flying and contaminating the instrument pipelines.
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High-Pressure Gas Adsorption 0-50/69Mpa

It can automatically conduct high-temperature and high-pressure gas adsorption and desorption isotherm tests, hydrogen storage PCT, hydrogen absorption and desorption, cyclic tests, etc. Designed to withstand pressures up to 69 MPa, the analyzer's robust pipeline and components are specifically engineered for demanding applications such as hydrogen storage, unconventional oil and gas recovery, and other high-pressure gas studies. This ensures reliable, precise results in a wide range of industrial and research settings.

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Full Automation

The analyzer offers complete automation from sample pre-treatment to adsorption testing, utilizing an in-situ degassing system and a reliable platform switching mechanism. This streamlined design eliminates the need for manual intervention during lengthy activation and testing processes, allowing testers to focus on analysis rather than operation. The system also supports cyclic adsorption and desorption tests, enabling the evaluation of material durability while significantly reducing repetitive tasks and saving valuable time for users.

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High Safety Design

Designed with safety as a top priority, the analyzer incorporates all-pneumatic valves, eliminating the need for solenoid valves, and ensuring enhanced reliability and performance at high safety standards. The instrument is equipped with two high-sensitivity combustible gas detection alarms—one inside and one outside—offering detection limits better than 3% LEL, providing real-time monitoring for hazardous conditions. Additionally, the analysis position is safeguarded by a protective cover, which prevents exposure to high temperatures, ensuring operator safety. This cover also minimizes the impact of external airflow fluctuations, significantly improving test accuracy and the overall stability of the instrument.

Other Feature

The analyzer is equipped with dual flammable gas detection alarms—one inside and one outside the system—for enhanced safety and real-time hazard monitoring. Additionally, the analysis position features a protective cover to shield operators from high temperatures, ensuring full protection during testing.

The instrument incorporates a patented BEST manifold design, providing exceptional integrity and minimizing dead volume to improve measurement accuracy. The all-stainless-steel gas pipeline system utilizes VCR metal hard connectors for superior sealing, and leak detection is conducted with an Inficon helium mass spectrometer, ensuring a high level of system airtightness and reliability.

Equipped with an imported high-precision pressure sensor, the system offers an impressive accuracy of 0.01% FS and long-term stability of 0.025% FS, ensuring precise pressure measurements over extended periods of use.

A non-barrier pollution prevention device, combined with an anti-pumping software program, eliminates the risk of volatile sample boiling under high vacuum conditions. This design prevents contamination of the valve and pipeline system, preserving the integrity and airtightness of the entire system.

The standard sample tube filling rod is equipped with a filter to reduce the free space volume in the sample tube. This effectively prevents sample splashing or contamination of the instrument's internal components, safeguarding both the instrument and the integrity of the test.

Typical Cases & Paper Citation

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