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BSD-PHE AUTOMATIC HIGH PRESSURE ADSORPTION KINETICS ANALYZER

The BSD PHE High-Pressure Adsorption Kinetics Analyzer is a fully automated, high-efficiency instrument designed for precise gas adsorption analysis under high-pressure conditions. It offers advanced kinetics analysis at isobaric high pressure, making it an ideal and cost-effective alternative to traditional magnetic balance gravimetric analyzers.The system features an optional TPD (Temperature Programmed Desorption) module for programmed temperature desorption, as well as capabilities for hydrogen absorption and desorption kinetics testing. It also supports TPD desorption rate analysis, platform temperature control, and TPA (Temperature Programmed Absorption) hydrogen absorption rate testing, providing comprehensive insights into material behavior under varying temperature and pressure conditions.With its versatile testing options and high level of automation, the BSD PHE Analyzer delivers reliable, accurate results for a wide range of high-pressure adsorption and desorption applications.

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Key Feature

Pressure

0-20MPa

Temperature

-196℃ to 1100℃

Main Function

Kinetics, High pressure Isotherm, PCT, Automatic Cyclic Test

Optional Function

TPD, TPA,
PCT with larger sample volume (100g level)

Full Automation

Automatically switches from pre-treatment to testing

Thermostatic design

The analyzer pipeline temperature is 40.0℃ ±0.1℃.

Sample cell options

Stainless steel sample cell :2ml/ 5ml/25ml;
Core sample cell:Φ25.4×50mm/Φ50×110mm/Φ38.1×100mm

High-pressure design

All stainless steel gas circuit system, the joints are hard-connected with VCR, which improves the stability of the instrument.

Transducers

High precision with 0.01%FS, long term 0.025%FS；

Specifications

Specifications	Details
Main Function	High pressure adsorption and desorption isotherm High pressure PCT Automatic Cyclic Test Isobaric pressure adsorption/desorption kinetics
Optional Function	Temperature programmed desorption (TPD) Temperature programmed adsorption (TPA) Vacuum desorption PCT test with larger sample volume (100g level)
Analysis station	1
Degassing station	1 in situ
Pressure	0-20MPa
Temperature	-196 to 1100℃
Transducer	2x pcs 10bar and 200bar with 0.01% full scale
Vacuum	10-2 Pa by oil pump 10-8 Pa by molecular pump
Analysis gas	H2、CH4、Ar、CO2、N2、Kr、O2、C2H6、C2H4、He etc.
Repeatability	±2% by standard sample
Sample cell	Stainless steel sample cell :2ml/ 5ml/25ml; Core sample cell:Φ25.4×50mm/Φ50×110mm/Φ38.1×100mm Self-sealing sample tube
Automation	Automatically switches from pre-treatment to testing after setup
Instrument thermostatic temperature	The inside of the instrument is in the same air bath environment, the thermostatic temperature is 40.0℃, and the temperature control accuracy is ±0.1℃.
High-pressure gas pipeline	All stainless steel gas circuit system, the joints are hard-connected with VCR, which improves the stability of the instrument.
Filling rod with filter	Standard sample tube filling rod with filtering function can effectively reduce the free space volume of the sample tube and prevent the sample from flying and contaminating the instrument pipelines.

High-Pressure Adsorption Kinetics 0-20Mpa

It can automatically conduct high-temperature and high-pressure gas adsorption and desorption isotherm tests, hydrogen storage PCT, hydrogen absorption and desorption, cyclic tests, etc. Designed to withstand pressures up to 20 MPa, the analyzer's robust pipeline and components are specifically engineered for demanding applications such as hydrogen storage, unconventional oil and gas recovery, and other high-pressure gas studies. High pressure Isobaric kinetics function will be a cost-effective alternative to traditional magnetic balance gravimetric analyzers.

Full Automation

The analyzer offers complete automation from sample pre-treatment to adsorption testing, utilizing an in-situ degassing system and a reliable platform switching mechanism. This streamlined design eliminates the need for manual intervention during lengthy activation and testing processes, allowing testers to focus on analysis rather than operation. The system also supports cyclic adsorption and desorption tests, enabling the evaluation of material durability while significantly reducing repetitive tasks and saving valuable time for users.

High Safety Design

Designed with safety as a top priority, the analyzer incorporates all-pneumatic valves, eliminating the need for solenoid valves, and ensuring enhanced reliability and performance at high safety standards. The instrument is equipped with two high-sensitivity combustible gas detection alarms—one inside and one outside—offering detection limits better than 3% LEL, providing real-time monitoring for hazardous conditions. Additionally, the analysis position is safeguarded by a protective cover, which prevents exposure to high temperatures, ensuring operator safety. This cover also minimizes the impact of external airflow fluctuations, significantly improving test accuracy and the overall stability of the instrument.

Other Feature

The analyzer is equipped with dual flammable gas detection alarms—one inside and one outside the system—for enhanced safety and real-time hazard monitoring. Additionally, the analysis position features a protective cover to shield operators from high temperatures, ensuring full protection during testing.

The instrument incorporates a patented BEST manifold design, providing exceptional integrity and minimizing dead volume to improve measurement accuracy. The all-stainless-steel gas pipeline system utilizes VCR metal hard connectors for superior sealing, and leak detection is conducted with an Inficon helium mass spectrometer, ensuring a high level of system airtightness and reliability.

Equipped with an imported high-precision pressure sensor, the system offers an impressive accuracy of 0.01% FS and long-term stability of 0.025% FS, ensuring precise pressure measurements over extended periods of use.

A non-barrier pollution prevention device, combined with an anti-pumping software program, eliminates the risk of volatile sample boiling under high vacuum conditions. This design prevents contamination of the valve and pipeline system, preserving the integrity and airtightness of the entire system.

The standard sample tube filling rod is equipped with a filter to reduce the free space volume in the sample tube. This effectively prevents sample splashing or contamination of the instrument's internal components, safeguarding both the instrument and the integrity of the test.